supercritical fluid methods for coal extraction

A Procedure for the Supercritical Fluid Extraction of Coal

A Procedure for the Supercritical Fluid Extraction of Coal Samples, with Subsequent Analysis of Extracted Hydrocarbons By Jonathan J. Kolak Introduction This report provides a detailed, step-by-step procedure for conducting extractions with supercritical carbon dioxide (CO 2) using the ISCO SFX220 supercritical fluid extraction system.

Supercritical fluid extraction of coal

publications where its used for supercritical extraction of coal at present day[1, 2]. The main goal of the authors in the first article on this subject was to study an opportunity to use this method for separation of co-products of coal. For better extraction authors propose to increase the pressure of the process and to grind coal to a powder[3].

Supercritical fluid extraction of coal under pyrolysis

Apr 01, 1994 (Keywords: supercritical fluid extraction; coal; pyrolysis) The supercritical fluid extraction technique was first applied to coal liquefaction by the National Coal Board of England about 20 years ago1. The extraction of coals under pyrolysis conditions using supercritical solvents has been studied1 13 since then due to its unique

New method for the direct analysis of supercritical fluid

Apr 01, 1983 The extraction process was observed as a function of pressure to determine threshold pressures for individual solutes or as a function of temperature at constant pressure. The method was demonstrated for a supercritical fluid extraction of a bituminous coal by a mixture of n-pentane and 2-propanol at 280 °C and 0.5–10 MPa.

SUPERCRITICAL FLUID EXTRACTION MedXtractor

Supercritical fluid extraction is the most effective and efficient way to extract valuable constituent botanicals. Supercritical Fluid Extraction (SFE) is the process of separating one component (the extractant) from another (the matrix) using supercritical fluids that is CO 2 as the extracting solvent.

Supercritical fluid extraction and fractionation of high

Apr 01, 2010 The high-temperature coal tar sample was separated into 10 narrow oil fractions and one solid-phase pitch product by supercritical fluid extraction and fractionation using n-pentane as solvent at 220°C and pressure from 5 to 15 MPa.Results show that the accumulative yields increase with the extract pressure especially at the lower pressures, and the yield increase rate decrease gradually.

BENEFICIATION OF COAL USING SUPERCRITICAL WATER AND

dioxide (ScWC) all can effectively extract about 50% of total sulfur from bituminous coal in one hour. Extraction above 350℃ decreased effectiveness, and extraction above the supercritical point of pure water caused polymerization presumably due to hydrothermal carbonization. Elimination of organic sulfur may play a role in the polymerization.

Supercritical Fluid Extraction an overview

Supercritical Fluid Extraction. SFE is a highly selective method using pressurized fluids as solvents. A supercritical fluid originates from a fluid being forced to pressure and temperature that is above its critical point causing the liquid and gas phases to become indistinguishable from each other. Supercritical fluids exhibit physicochemical

Supercritical fluid methods: An alternative to

Mar 01, 2020 For several years, supercritical fluid-based preparation processes have been considered as a good alternative to conventional liposome preparation methods. A number of supercritical fluid processes allowing the liposome preparation are described depending on the role of the supercritical fluid with respect to the liposome raw materials.

Supercritical fluid extraction

Supercritical fluid extraction (SFE) is the process of separating one component (the extractant) from another (the matrix) using supercritical fluids as the extracting solvent. Extraction is usually from a solid matrix, but can also be from liquids. SFE can be used as a sample preparation step for analytical purposes, or on a larger scale to either strip unwanted material from a product (e.g. decaffeination) or collect a desired product (e.g. essential oils). These essential oils can include limonene and other straight solvents.

A Procedure for the Supercritical Fluid Extraction of Coal

A Procedure for the Supercritical Fluid Extraction of Coal Samples, with Subsequent Analysis of Extracted Hydrocarbons By Jonathan J. Kolak Introduction This report provides a detailed, step-by-step procedure for conducting extractions with supercritical carbon dioxide (CO 2) using the ISCO SFX220 supercritical fluid extraction system.

Supercritical fluid extraction of coal

publications where its used for supercritical extraction of coal at present day[1, 2]. The main goal of the authors in the first article on this subject was to study an opportunity to use this method for separation of co-products of coal. For better extraction authors propose to increase the pressure of the process and to grind coal to a powder[3].

Supercritical Fluid Extraction of REEs Using CO2 SBIR.gov

TDA Research, in collaboration with the Idaho National Laboratory, proposes to develop a new method to cost-effectively extract rare earth elements from domestically abundant coal and coal by-products using an environmentally friendly process. The new REE extraction process is based on a unique reactor design for supercritical CO2 extraction of

Supercritical fluid extraction of coal tar-contaminated

Soil samples containing coal tar residues from manufactured gas (town gas) plants were extracted by carbon dioxide supercritical fluid extraction (SFE) and Soxhlet extraction techniques. The detection limits and the reproducibility of the SFE method were evaluated, and the comparability of measured concentrations of polycyclic aromatic hydrocarbons (PAH) by the two extraction methods was

Energy and Environmental Research Emphasizing Low-Rank

Low-Rank Coal -- Task 4.4 Development of Supercritical Fluid Extraction Methods for the Quantitation of Sulfur Forms in Coal Topical Report Ronald C. Timpe Work Performed Under Contract No.: DE-FC21-93MC30097 For U.S. Department of Energy Office of Fossil Energy Morgantown Energy Technology Center P.O. Box 880 Morgantown, West Virginia 26507-0880

METHOD 3560 SUPERCRITICAL FLUID EXTRACTION OF

method is suitable for use wi th any supercritical fluid extraction (SFE) system that allows extraction conditions (e.g., pressure, temperature, flow rate) to be adjusted to achieve separation of the TRPHs from the matrices of concern. 1.2 Method 3560 is not suitable for the extraction

US4443321A Supercritical solvent coal extraction

Yields of soluble organic extract are increased up to about 50% by the supercritical extraction of particulate coal at a temperature below the polymerization temperature for coal extract fragments (450° C.) and a pressure from 500 psig to 5,000 psig by the conjoint use of a solvent mixture containing a low volatility, high critical temperature coal dissolution catalyst such as phenanthrene

Supercritical Fluid Extraction of Bioactive Compounds from

The purpose of plant material extraction is to obtain large amounts of extract rich in the desired active compounds in a time-sensitive and cost-effective manner. The productivity and profitability of a supercritical fluid extraction (SFE) process largely depends on the selection of process parameters, which are elaborated upon in this paper.

US Patent Application for EXPERIMENTAL METHOD FOR COAL

Nov 21, 2020 An experimental method for coal desulfurization and deashing using permeation and solvating power of a supercritical fluid includes the following steps. The coal sample is ground and loaded into an extraction kettle with a cover. An inlet valve and an outlet valve of the extraction kettle are opened to circulate the supercritical CO2 fluid in the extraction kettle.

Supercritical fluid extraction: fundamental principles and

Lookup at Google Scholar. Supercritical fluid extraction: fundamental principles and modeling methods. 1986. Rizvi, S.S.H.; Benado, A.L.; Zollweg, J.A.; Daniels, J.A. A review and critical evaluation is presented on the current understanding of supercritical fluid extraction (SFE) for unit processing operations for extracting food components

US4485003A Supercritical extraction and simultaneous

A process for producing liquid hydrocarbons from coal comprises treating comminuted coal at 380° to 600° C. and 260 to 450 bar with water in a high pressure reactor to form a charged supercritical gas phase and a coal residue. Simultaneously with the water treatment, hydrogenation with hydrogen takes place in the presence of a catalyst.

Coal liquefaction process streams characterization and

Jul 01, 1992 Characterization of coal-derived materials by field desorption mass spectrometry, two-dimensional nuclear magnetic resonance, supercritical fluid extraction, and supercritical fluid chromatography/mass spectrometry. United States: N. p., 1992. Web. doi:10.2172/10174665.

Supercritical fluid fractionation of petroleum- and coal

Supercritical fluid extraction / capillary supercritical fluid chromatography / Fourier transform infrared microspectrometry of polycyclic aromatic compounds in a coal tar pitch. Journal of High Resolution Chromatography 1988, 11 (11),766-775. DOI: 10.1002/jhrc.1240111105.

Supercritical fluid extraction SlideShare

Oct 14, 2014 Supercritical fluid extraction 1. SUPERCRITICAL FLUID EXTRACTION PRAGATI SINGHAM PhD (I Year) 2. CONTENTS • Introduction to SCF Properties of SCF Historical background • Supercritical fluid Extraction (SFE) Components of SFE Critical properties of selected substances Modes of SFE • Methods of developments of SFE • Objectives for commercialization • Advantages

A Procedure for the Supercritical Fluid Extraction of Coal

A Procedure for the Supercritical Fluid Extraction of Coal Samples, with Subsequent Analysis of Extracted Hydrocarbons By Jonathan J. Kolak Introduction This report provides a detailed, step-by-step procedure for conducting extractions with supercritical carbon dioxide (CO 2) using the ISCO SFX220 supercritical fluid extraction system.

Mechanism of supercritical fluid extraction of coal

This paper describes the mechanism of supercritical toluene (or toluene-tetralin mixture) extraction of coal. The effects of solvent power and solvent residence time in the cell on conversion and liquid yield were examined by using a two-stage extraction method: extraction at various conditions followed by high-solvent power extraction.

Principles of supercritical fluid systems (5) What is

Oct 06, 2020 Supercritical fluid extraction (SFE) is a method in which supercritical fluid as an extraction medium is added to substances containing target components, and extraction is performed based on differences in solubility. In particular, the use of supercritical carbon dioxide as an extraction medium offers many advantages in a variety of fields

Task 4.4 development of supercritical fluid extraction

Apr 01, 1995 This method has disproved the generally accepted idea that elemental sulfur is associated with the organic fraction. A paper reporting the results obtained on this subject entitled {open_quote}Determination of Elemental Sulfur in Coal by Supercritical Fluid Extraction and Gas Chromatography with Atomic Emission Detection{close_quote} was

Introduction to Supercritical Fluid Chromatography (The

Supercritical fluid extraction (SFE) is a method in which supercritical fluid as an extraction medium is added to substances containing target components, and extraction is performed based on differences in solubility. Coal, oil, energy Plastic, rubber, polymer Metal Inorganic compounds and ceramics Fig. 6 Configuration of supercritical

US4443321A Supercritical solvent coal extraction

Yields of soluble organic extract are increased up to about 50% by the supercritical extraction of particulate coal at a temperature below the polymerization temperature for coal extract fragments (450° C.) and a pressure from 500 psig to 5,000 psig by the conjoint use of a solvent mixture containing a low volatility, high critical temperature coal dissolution catalyst such as phenanthrene

Production of Mesophase Pitch from Coal Tar and Petroleum

Petroleum Pitches using Supercritical Fluid Extraction This method yielded similar results to traditional methods but has some advantages over them, as will be outlined later. Experimental The extraction system was used for the extraction of coal tar and Ashland-240 petroleum pitches.

Supercritical solvent coal extraction The United States

A method according to claim 6 in which the coal is present in the reactor in an amount of from 1 to 99% by weight of the total weight of coal and solvent. 8. A method according to claim 1 in which the reactor is heated to a temperature from 300° C. to 400° C. and a pressure from about 1,000 to 2,500 psig. the supercritical fluid

(PDF) Kinetics of extraction of coal-tar pitch components

Chemical analysis of coal tar related compounds is usually preceded by extraction from the sample matrix [7][8][9]. Supercritical fluid extraction (SFE) has become an accepted alternative to traditional solvent extraction methods [10,11]. The main advantages of SFE are the rate of extraction and the reduced amount of liquid solvent required [12

SUPERCRITICAL FLUID EXTRACTION OF VEGETABLE

Keywords: carbon dioxide, supercritical fluid extraction, vegetable materials. 1. Introduction A wide use of supercritical gas extraction (SGE) or supercritical fluid extraction (SFE), as an extraction or separation method, in fuel and energy, chemical, food production or pharmaceutical industries as well as

US4898673A Dynamic supercritical fluid extraction system

238000000194 supercritical-fluid extraction Methods 0.000 title 1 239000002904 solvent Substances 0.000 claims abstract description 84 239000007787 solid Substances 0.000 claims abstract description 65

Supercritical Fluids (SCF) Supercritical Fluid Extraction

Supercritical fluid extraction (SFE) plants are operating at throughputs of 100,000,000 lbs/yr or more in the foods industry. Coffee and tea are decaffeinated via supercritical fluid extraction and most major brewers in the US and Europe use flavors that are extracted from hops with supercritical fluids.

Supercritical fluid extraction

Supercritical fluid extraction (SFE) is the process of separating one component (the extractant) from another (the matrix) using supercritical fluids as the extracting solvent.Extraction is usually from a solid matrix, but can also be from liquids.SFE can be used as a sample preparation step for analytical purposes, or on a larger scale to either strip unwanted material from a product (e.g

Supercritical fluid extraction and similar topics

A few laboratory test methods include the use of supercritical fluid extraction as an extraction method instead of using traditional solvents. Supercritical fluid For example, supercritical carbon dioxide is used to extract caffeine in the manufacture of decaffeinated coffee.

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